IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

Base Information

Chemical Name:IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2
CAS No.:66350-34-3
Molecular Formula:2BF₄*C₅₃H₄₉IrOP₄
Molecular Weight:1191.7
Hs Code.:

IrH(CO)(((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)2)2<sup>(2+)</sup>*2BF<sub>4</sub><sup>(1-)</sup> = [IrH(CO)(((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)2)2](BF<sub>4</sub>)2

Synonyms:IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

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Chemical Property of IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

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Technology Process of IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

There total 4 articles about IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 15130-28-6
[Ir(κ²-P,P-1,2-bis(diphenylphosphino)ethane)₂]BF₄

: 66350-34-3
IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

Guidance literature:: With CO; In dichloromethane; HBF4*(C2H5)2O (slight excess) added to Ir complex soln., CO bubbled; ether added, filtered, recrystd. (CH2Cl2/THF);

Reference yield: 60.0%

: 13826-83-0
ammonium tetrafluroborate

: 15390-38-2,15131-25-6
bis(1,2-bis(diphenylphosphino)ethane)iridium(I) chloride

: 66350-34-3
IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

Guidance literature:: With CO; HCl; In dichloromethane; Ir complex soln. satd. with CO, HCl bubbled, pptd. (THF), filtered, washed (THF), dried (vac.), treated with NH4BF4 (metathesis); recrystd. (CH2Cl2/Et2O); elem. anal.;

Reference yield:

: 91685-23-3
IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

: 66350-34-3
IrH(CO)(((C₆H₅)2PCH₂)2)2⁽²⁺⁾*2BF₄^(1-) = [IrH(CO)(((C₆H₅)2PCH₂)2)2](BF₄)2

Guidance literature:: With water; In [⁽²⁾H₆]acetone; byproducts: H3O(1+), H2O; (N2), complex dissolved, H2O added; not isolated, detected by NMR;
DOI:10.1021/om00122a029