Technology Process of C42H35BN2O2
There total 5 articles about C42H35BN2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
1,4-dioxane;
at 95 ℃;
for 24h;
- Guidance literature:
-
(9,9’-(5-(4,4,5,5-tetramethyl-1,2,3-dioxaborolan-2-yl)-1,3-phenylene)bis(9H-carbazole)); 1.4-dibromobenzene;
With
potassium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; water; toluene;
for 24h;
Inert atmosphere;
Reflux;
With
n-butyllithium;
In
tetrahydrofuran; hexane; water; toluene;
at -70 ℃;
for 0.5h;
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane;
In
tetrahydrofuran; hexane; water; toluene;
at -70 - 20 ℃;
for 7h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; copper(l) chloride / dimethyl sulfoxide / 8 h / Reflux; Inert atmosphere
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -70 - 40 °C / Inert atmosphere
2.2: 7 h / -70 - 20 °C
3.1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; water; tetrahydrofuran / 24 h / Inert atmosphere; Reflux
3.2: 0.5 h / -70 °C
3.3: 7 h / -70 - 20 °C
With
n-butyllithium; potassium carbonate; copper(l) chloride;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; hexane; water; dimethyl sulfoxide; toluene;
