1,4-Bisiodo>benzene

Base Information

• Chemical Name: 1,4-Bisiodo>benzene
• CAS No.: 1026186-30-0
• Molecular Formula: C₂₀H₁₄F₆I₂O₆S₂
• Molecular Weight: 782.259

Synonyms:1,4-Bisiodo>benzene

Chemical Property of 1,4-Bisiodo>benzene

Chemical Property:

Purity/Quality:

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Technology Process of 1,4-Bisiodo>benzene

There total 2 articles about 1,4-Bisiodo>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluorormethanesulfonic acid (1493-13-6) + iodosylbenzene (536-80-1) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → cis-1,2-cyclohexanediyl 1,2-bis(trifluoromethanesulfonate) (91146-10-0) + 1,4-Bisiodo>benzene (1026186-30-0)

Guidance literature:

Yield given. Multistep reaction; 1) CH₂Cl₂, 3 h, r.t., 2) 2 h;

DOI:10.1021/jo00051a025

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + iodosylbenzene (536-80-1) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → cis-1,2-cyclohexanediyl 1,2-bis(trifluoromethanesulfonate) (91146-10-0) + 1,4-Bisiodo>benzene (1026186-30-0)

Guidance literature:

Yield given. Multistep reaction; 1) CH₂Cl₂, 3 h, r.t., 2) 2 h;

DOI:10.1021/jo00051a025

Reference yield: 100.0%

diphenyl sulfide (139-66-2) + 1,4-Bisiodo>benzene (1026186-30-0) → (p-Phenylene)bis(diphenylsulfonium) ditriflate (144767-83-9)

Guidance literature:

With copper diacetate; at 200 ℃; for 0.5h;

DOI:10.1021/jo00051a025

upstream raw materials:

trifluorormethanesulfonic acid

iodosylbenzene

benzene

trifluoromethylsulfonic anhydride

Downstream raw materials:

(p-Phenylene)bis(diphenylsulfonium) ditriflate

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