(2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

Base Information

Chemical Name:(2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol
CAS No.:214134-42-6
Molecular Formula:C₂₉H₃₃NO₅
Molecular Weight:475.585
Hs Code.:

Synonyms:(2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

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Chemical Property of (2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

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Technology Process of (2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

There total 6 articles about (2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-24-7
acetic anhydride

: 87984-35-8
(2-L-1,3/2,4,5)-1-amino-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

: 214134-42-6
(2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

Guidance literature:: In methanol; for 8h; Ambient temperature; 1.) 0 deg C;
DOI:10.1016/S0040-4039(98)01428-2

Reference yield:

: 214134-40-4
(2-L-1,3/2,4,5)-1-(benzyloxy)amino-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

: 214134-42-6
(2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NiCl₂*6H₂O; NaBH₄ / methanol / 8 h / -10 °C

2: 90 percent / methanol / 4 h / 20 °C

With sodium tetrahydroborate; nickel dichloride; In methanol;
DOI:10.1081/CAR-120026471

Reference yield:

: 87940-06-5,87984-32-5
(2R,3S,4S,5S)-2,3,4-Tris-benzyloxy-5-hydroxy-cyclohexanone oxime

: 214134-42-6
(2-L-1,3/2,4,5)-1-acetamido-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 1.) NaH / dimethylformamide / 24 h / 100 °C / 1.) 0 deg C

2: 74 percent / LiAlH₄ / tetrahydrofuran / 12 h / Heating

3: 90 percent / methanol / 8 h / Ambient temperature; 1.) 0 deg C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)01428-2