(2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Base Information

Chemical Name:(2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol
CAS No.:651325-22-3
Molecular Formula:C₃₆H₃₈N₂O₅
Molecular Weight:578.708
Hs Code.:

Synonyms:(2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Suppliers and Price of (2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

There total 6 articles about (2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 651325-21-2
(2-L-1,3/2,4)-1-acetamido-5-oxo-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

: 651325-22-3
(2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Guidance literature:: With pyridine; In methanol; at 20 ℃; for 2h;
DOI:10.1081/CAR-120026471

Reference yield:

: (2R,3S,4S,5S)-2,3,4-Tris-benzyloxy-5-hydroxy-cyclohexanone oxime

: 651325-22-3
(2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / NaH / dimethylformamide / 3 h / 90 °C

2: 74 percent / LiAlH₄ / tetrahydrofuran / 12 h / Heating

3: 90 percent / methanol / 4 h / 20 °C

4: 86 percent / PCC / CH₂Cl₂ / 48 h / 20 °C

5: 100 percent / pyridine / methanol / 2 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-120026471

Reference yield:

: 651325-18-7
(2-L-2,4,5/3)-1-benzyloxyimino-2,3,4-tri-O-benzyl-2,3,4,5-cyclohexanetetrol

: 651325-22-3
(2-L-1,3/2,4)-1-acetamido-5-(benzyloxy)imino-2,3,4-tri-O-benzyl-2,3,4-cyclohexanetriol

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / LiAlH₄ / tetrahydrofuran / 12 h / Heating

2: 90 percent / methanol / 4 h / 20 °C

3: 86 percent / PCC / CH₂Cl₂ / 48 h / 20 °C

4: 100 percent / pyridine / methanol / 2 h / 20 °C

With pyridine; lithium aluminium tetrahydride; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1081/CAR-120026471