Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI)

Base Information

Chemical Name:Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI)
CAS No.:397266-08-9
Molecular Formula:C₇H₁₀O₃
Molecular Weight:142.155
Hs Code.:
Mol file:397266-08-9.mol

Synonyms:Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI)

Suppliers and Price of Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI)

Chemical Property:

PSA：43.37000
LogP:0.38450

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI)

There total 5 articles about Cyclopropanecarboxaldehyde, 2-[(acetyloxy)methyl]-, (1S,2S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1411940-90-3
(4S,5S)-diisopropyl-2-((1S,2S)-2-(acetoxymethyl)cyclopropyl)-1,3-dioxoline-4,5-dicarboxylate

: 397266-08-9,397274-64-5
((1S*,2S*)-2-formylcyclopropyl)methyl acetate

Guidance literature:: With acetic acid; at 80 ℃; for 2h;

Reference yield:

: 38982-39-7
acetic acid trans-4-oxo-but-2-enyl ester

: 397266-08-9,397274-64-5
((1S*,2S*)-2-formylcyclopropyl)methyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium nitrate / ethanol / 15 h / 20 °C

2: pyridinium p-toluenesulfonate / benzene / 15 h / 90 °C

3: diethylzinc / hexane / 8 h / -20 - 20 °C / Inert atmosphere

4: acetic acid / 2 h / 80 °C

With diethylzinc; acetic acid; ammonium nitrate; pyridinium p-toluenesulfonate; In ethanol; hexane; benzene;

Reference yield:

: 27977-16-8,64196-68-5,70940-89-5
trans-1-hydroxy-4-acetoxy-2-butene

: 397266-08-9,397274-64-5
((1S*,2S*)-2-formylcyclopropyl)methyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: manganese(IV) oxide / dichloromethane / 48 h / 20 °C

2: ammonium nitrate / ethanol / 15 h / 20 °C

3: pyridinium p-toluenesulfonate / benzene / 15 h / 90 °C

4: diethylzinc / hexane / 8 h / -20 - 20 °C / Inert atmosphere

5: acetic acid / 2 h / 80 °C

With manganese(IV) oxide; diethylzinc; acetic acid; ammonium nitrate; pyridinium p-toluenesulfonate; In ethanol; hexane; dichloromethane; benzene;