benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

Base Information

Chemical Name:benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester
CAS No.:78578-11-7
Molecular Formula:C₃₅H₃₂N₄O₁₁
Molecular Weight:684.659
Hs Code.:

Synonyms:benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

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Chemical Property of benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

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Technology Process of benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

There total 6 articles about benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 78596-98-2
(S)-4-Benzyloxycarbonylamino-4-[(S)-1-(4-nitro-benzyloxycarbonyl)-2-phenyl-ethylcarbamoyl]-butyric acid

: 78578-11-7
benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃;

Reference yield:

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 78578-11-7
benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / Et₃N / dimethylformamide / 72 h / Ambient temperature

2: 42 percent / LiOH*0.5 H₂O / acetone; H₂O / 3 h / 40 °C

3: 99 percent / Et₃N / dimethylformamide / Ambient temperature

4: 90 percent / trifluoroacetic acid, anisole / 1 h / Ambient temperature

5: 99 percent / N,N'-dicyclohexycarbodiimide, pyridine / dimethylformamide / 0 °C

With pyridine; lithium hydroxide; methoxybenzene; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 27442-37-1
L-Phenylalanin-p-nitro-benzylester

: 78578-11-7
benzyloxycarbonyl-γ-p-nitrophenyl-L-glutamyl-L-phenylalanine p-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / dimethylformamide / Ambient temperature

2: 90 percent / trifluoroacetic acid, anisole / 1 h / Ambient temperature

3: 99 percent / N,N'-dicyclohexycarbodiimide, pyridine / dimethylformamide / 0 °C

With pyridine; methoxybenzene; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;