2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

Base Information

Chemical Name:2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione
CAS No.:114506-70-6
Molecular Formula:C₂₀H₂₆O₄
Molecular Weight:330.424
Hs Code.:

Synonyms:2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

Suppliers and Price of 2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

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Technology Process of 2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

There total 1 articles about 2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 823-36-9
2-ethylcyclopentane-1,3-dione

: 56475-35-5
5-Methoxy-3-(4-methoxy-phenyl)-pent-1-en-3-ol

: 114506-70-6
2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In xylene; Heating;
DOI:10.1021/jo00249a010

Reference yield: 43.0%

: 114506-70-6
2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

: 114506-75-1
7a-ethyl-3a-hydroxy-5-(p-methoxyphenyl)-2β,3,3aβ,4β,7,7aβ-hexahydro-2,4-methano-1H-inden-1-one

: 114506-74-0
5-ethyl-2-exo-(2-methoxyethyl)-2-endo-(p-methoxyphenyl)bicyclo<3.2.1>octane-6,8-dione

Guidance literature:: With hydrogenchloride; In methanol; for 4h; Ambient temperature;
DOI:10.1021/jo00249a010

Reference yield:

: 114506-70-6
2-ethyl-2-<5-methoxy-3-(p-methoxyphenyl)pent-2-enyl>cyclopentane-1,3-dione

: 111015-11-3,114579-42-9,114579-47-4
7a-ethyl-5-(p-methoxyphenyl)-1-methyl-(2β,3aβ,4β,5β,7aβ)-octahydro-2,4-methano-1H-indene-1,3a-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 28 percent / HCl gas / methanol / 4 h / Ambient temperature

2: 98 percent / H₂ / 10percent Pd-C / methanol

3: 95 percent / diethyl ether; tetrahydrofuran / 1.) RT, 2 h, 2.) reflux, 30 min

With hydrogenchloride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1021/jo00249a010