4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

Base Information

Chemical Name:4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt
CAS No.:1445862-54-3
Molecular Formula:C₄H₁₁N*C₂₃H₂₃ClN₂O₅S
Molecular Weight:548.103
Hs Code.:

Synonyms:4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

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Chemical Property of 4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

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Technology Process of 4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

There total 8 articles about 4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3144-09-0
methanesulfonamide

: 1445862-74-7
4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)benzaldehyde

: 109-89-7
diethylamine

: 1445862-54-3
4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

Guidance literature:: methanesulfonamide; 4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)benzaldehyde; With bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene; In Isopropyl acetate; at 20 ℃; for 2h; Inert atmosphere;

diethylamine;

Reference yield:

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 1445862-54-3
4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 7 h / 80 °C / Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 18 h / 80 °C / Inert atmosphere

3: bis(tertbutylcarbonyloxy)iodobenzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} / Isopropyl acetate / 2 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene; potassium carbonate; caesium carbonate; In 1,4-dioxane; Isopropyl acetate; water; dimethyl sulfoxide;

Reference yield:

: 848243-23-2
2-ethoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

: 1445862-54-3
4-(3-chloro-4-ethylphenoxy)-3-(2-ethoxypyridin-3-yl)-N-(methylsulfonyl)benzamide diethylamine salt

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 7 h / 80 °C / Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 18 h / 80 °C / Inert atmosphere

3: bis(tertbutylcarbonyloxy)iodobenzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} / Isopropyl acetate / 2 h / 20 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; bis(tertbutylcarbonyloxy)iodobenzene; potassium carbonate; caesium carbonate; In 1,4-dioxane; Isopropyl acetate; water; dimethyl sulfoxide;