1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

Base Information

Chemical Name:1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride
CAS No.:1360468-64-9
Molecular Formula:C₂₂H₃₀N₃*Cl
Molecular Weight:371.953
Hs Code.:

Synonyms:1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

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Chemical Property of 1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

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Technology Process of 1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

There total 3 articles about 1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 875872-11-0
1-(1-methyl-2-dimethylaminoethyl)benzimidazole

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 1360468-64-9
1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 25 - 60 ℃; for 13h; Inert atmosphere;
DOI:10.1080/00958972.2012.654469

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1360468-64-9
1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 1 h / 20 °C

1.2: 6 h / Reflux

2.1: N,N-dimethyl-formamide / 20 h / 20 - 80 °C

With potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2020.127802

Reference yield:

: 108-14-5
2-chloro-1-dimethylaminopropane

: 1360468-64-9
1-(1-methyl-2-dimethylaminoethyl)-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 1 h / 20 °C

1.2: 6 h / Reflux

2.1: N,N-dimethyl-formamide / 20 h / 20 - 80 °C

With potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.molstruc.2020.127802