1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

Base Information

Chemical Name:1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone
CAS No.:1182277-94-6
Molecular Formula:C₂₅H₃₃NO₃Si
Molecular Weight:423.627
Hs Code.:

Synonyms:1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

Suppliers and Price of 1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

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Technology Process of 1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

There total 1 articles about 1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1182277-93-5
1-[(1R)-1-(tert-butyldiphenylsilyloxymethyl)-2-propenyl]-2,6-piperidinedione

: 1182277-94-6
1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

Guidance literature:: 1-[(1R)-1-(tert-butyldiphenylsilyloxymethyl)-2-propenyl]-2,6-piperidinedione; With lithium triethylborohydride; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

With dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; at -78 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo901059n

Reference yield:

: 1182277-94-6
1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-6-hydroxyhexahydro-2-pyridinone

: 1182277-98-0
1-[(1R)-1-(1-tert-butyldiphenylsilyloxymethyl)-2-propenyl]-1,2,3,4-tetrahydro-2-pyridinone

Guidance literature:: With triisopropyl-(4-vinyl-furan-2-yloxy)-silane; triisopropylsilyl trifluoromethanesulfonate; In diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo901059n