1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

Base Information

Chemical Name:1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol
CAS No.:881657-29-0
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:

Synonyms:1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

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Chemical Property of 1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

Chemical Property:

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Technology Process of 1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

There total 2 articles about 1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1398569-78-2
2-Amino-1,5-anhydro-2,3,4-trideoxy-D-erythro-hexitol hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 881657-29-0
1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

Guidance literature:: With sodium hydroxide; In water; at 0 - 20 ℃; for 16h;

Reference yield:

: 603130-12-7
1,5-anhydro-2-[(tert-butoxycarbonyl)amino]-2,3,4-trideoxy-D-erythro-hexitol

: 881657-29-0
1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; methanol / 1 h / 20 °C

2: sodium hydroxide / water / 16 h / 0 - 20 °C

With hydrogenchloride; sodium hydroxide; In 1,4-dioxane; methanol; water;

Reference yield:

: 881657-29-0
1,5-Anhydro-2-{[(benzyloxy)carbonyl]amino}-2,3,4-trideoxy-D-erythro-hexitol

: (4'S,5'R)-6-chloro-4'-(2-chloro-3-fluoropyridin-4-yl)-1'-[(1R,2S)-2-hydroxy-1,2-diphenylethyl]-N-[(3R,6S)-6-(hydroxymethyl)tetrahydro-2H-pyran-3-yl]-4,4-dimethyl-2-oxo-1,2-dihydrodispiro[cyclohexane-1,2'-pyrrolidine-3',3-indole]-5'-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 4 h / 20 °C

2: triethylamine / methanol / 120 h / 50 °C

With hydrogen; triethylamine; palladium 10% on activated carbon; In methanol;