Fe⁽²⁺⁾*(C₅H₄NCH₂)3N*(C₆H₅COCOO)^(1-)*ClO₄^(1-)={Fe((C₅H₄NCH₂)3N)(C₆H₅COCOO)}(ClO₄)

Base Information

• Chemical Name: Fe⁽²⁺⁾*(C₅H₄NCH₂)3N*(C₆H₅COCOO)^(1-)*ClO₄^(1-)={Fe((C₅H₄NCH₂)3N)(C₆H₅COCOO)}(ClO₄)
• CAS No.: 143294-11-5
• Molecular Formula: C₈H₅O₃*C₁₈H₁₈N₄*ClO₄*Fe
• Molecular Weight: 594.791

Synonyms:Fe⁽²⁺⁾*(C₅H₄NCH₂)3N*(C₆H₅COCOO)^(1-)*ClO₄^(1-)={Fe((C₅H₄NCH₂)3N)(C₆H₅COCOO)}(ClO₄)

Chemical Property of Fe⁽²⁺⁾*(C₅H₄NCH₂)3N*(C₆H₅COCOO)^(1-)*ClO₄^(1-)={Fe((C₅H₄NCH₂)3N)(C₆H₅COCOO)}(ClO₄)

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Technology Process of Fe⁽²⁺⁾*(C₅H₄NCH₂)3N*(C₆H₅COCOO)^(1-)*ClO₄^(1-)={Fe((C₅H₄NCH₂)3N)(C₆H₅COCOO)}(ClO₄)

There total 3 articles about Fe⁽²⁺⁾*(C₅H₄NCH₂)3N*(C₆H₅COCOO)^(1-)*ClO₄^(1-)={Fe((C₅H₄NCH₂)3N)(C₆H₅COCOO)}(ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

iron(II) perchlorate hexahydrate + tris[(2-pyridylmethyl)amine] (16858-01-8) + Benzoylformic acid (611-73-4) → Fe(2+)*(C5H4NCH2)3N*(C6H5COCOO)(1-)*ClO4(1-)={Fe((C5H4NCH2)3N)(C6H5COCOO)}(ClO4) (143294-11-5)

Guidance literature:

With N(C₂H₅)3; In methanol; mixing equimol. amounts of Fe(ClO4)2, ligands, and NEt3 in MeOH under Ar; cooling, filtration, elem. anal.;

Reference yield:

sodium benzoylformate (43165-51-1) + tris[(2-pyridylmethyl)amine] (16858-01-8) → (C18H18N4)Fe(C6H5C(O)COO)(1+)*ClO4(1-)=[(C18H18N4)Fe(C6H5C(O)COO)]ClO4 (143294-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (C₂H₅)3N / methanol

With (C₂H₅)3N; In methanol;

Reference yield:

(C18H18N4)Fe(C6H5C(O)COO)(1+)*ClO4(1-)*CH3OH=[(C18H18N4)Fe(C6H5C(O)COO)](ClO4)*CH3OH (163236-08-6) → (C18H18N4)Fe(C6H5C(O)COO)(1+)*ClO4(1-)=[(C18H18N4)Fe(C6H5C(O)COO)]ClO4 (143294-11-5)

Guidance literature:

drying (vacuum); elem. anal.;

upstream raw materials:

tris[(2-pyridylmethyl)amine]

Benzoylformic acid

(C₁₈H₁₈N₄)Fe(C₆H₅C(O)COO)⁽¹⁺⁾*ClO₄^(1-)*CH₃OH=[(C₁₈H₁₈N₄)Fe(C₆H₅C(O)COO)](ClO₄)*CH₃OH

sodium benzoylformate

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