8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone

Base Information

• Chemical Name: 8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone
• CAS No.: 61898-89-3
• Molecular Formula: C₂₇H₃₁N₅O₅
• Molecular Weight: 505.574

Synonyms:8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone

Chemical Property of 8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone

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Technology Process of 8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone

There total 1 articles about 8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.6%

(S)-Pyrrolidine-2-carboxylic acid [(S)-1-({[(S)-1-(hydrazinocarbonylmethyl-carbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-carbamoyl)-2-phenyl-ethyl]-amide; hydrochloride (82247-65-2) → 8,14-dibenzyl-dodecahydro-3a,6,9,12,15-pentaaza-cyclopentacyclopentadecene-4,7,10,13,16-pentaone (61898-89-3) + (6S,12S,15S,24S,30S,33S)-6,12,24,30-Tetrabenzyl-1,4,7,10,13,19,22,25,28,31-decaaza-tricyclo[31.3.0.015,19]hexatriacontane-2,5,8,11,14,20,23,26,29,32-decaone (82247-64-1)

Guidance literature:

With sodium nitrite; In water; N,N-dimethyl-formamide; at -15 ℃; for 0.5h;

DOI:10.1021/ja00381a006

upstream raw materials:

(S)-Pyrrolidine-2-carboxylic acid [(S)-1-({[(S)-1-(hydrazinocarbonylmethyl-carbamoyl)-2-phenyl-ethylcarbamoyl]-methyl}-carbamoyl)-2-phenyl-ethyl]-amide; hydrochloride

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