Technology Process of Pt(CH3)CO((OCH3)3C6H2NCCH3)2(1+)*BF4(1-)=PtCH3CO((OCH3)3C6H2NCCH3)2BF4
There total 1 articles about Pt(CH3)CO((OCH3)3C6H2NCCH3)2(1+)*BF4(1-)=PtCH3CO((OCH3)3C6H2NCCH3)2BF4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
water;
to suspn. of Pt-complex in trifluoroethanol was added aq. soln. of HBF4,stirred at room temp. for few min, flask was degassed and filled with 1 atm of CO, stirred under 1 atm of CO for 24 h; solvent was removed at -20°C to 0°C in vacuo, petroleum ether was added, dried for 30 min; elem. anal.;
DOI:10.1021/ja011189x