[2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester

Base Information

• Chemical Name: [2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester
• CAS No.: 262368-49-0
• Molecular Formula: C₁₄H₂₁N₃O₃
• Molecular Weight: 279.339
• Mol file: 262368-49-0.mol

Synonyms:[2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester

Chemical Property of [2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester

There total 1 articles about [2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2-[[(3-nitrophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester (892413-76-2) → [2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester (262368-49-0)

Guidance literature:

With thiophene; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; methanol;

Reference yield:

[2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester (262368-49-0) + 3-[[5-cyano-2-(methylthio)-4-pyrimidinyl]amino]-benzoic acid 1,1-dimethylethyl ester (892413-67-1) → 3-[[5-cyano-2-[[3-[[[[[(1,1-dimethylethoxy)carbonyl]amino]acetyl]amino]methyl]phenyl]amino]-4-pyrimidinyl]amino]-benzoic acid 1,1-dimethylethyl ester

Guidance literature:

3-[[5-cyano-2-(methylthio)-4-pyrimidinyl]amino]-benzoic acid 1,1-dimethylethyl ester; With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 2h;

[2-[[(3-aminophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester; In dichloromethane; at 20 - 60 ℃; for 1h;

upstream raw materials:

[2-[[(3-nitrophenyl)methyl]amino]-2-oxoethyl]-carbamic acid 1,1-dimethylethyl ester