Technology Process of C26H21NO2(18)O
There total 4 articles about C26H21NO2(18)O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,4-diaza-bicyclo[2.2.2]octane; 1,10-Phenanthroline; oxygen; 18O-labeled water; copper dichloride;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 4h;
under 760.051 Torr;
Mechanism;
DOI:10.1021/ol300896h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Petroleum ether / 10 h / Reflux
2: 1,4-diaza-bicyclo[2.2.2]octane; 1,10-Phenanthroline; oxygen; 18O-labeled water; copper dichloride / N,N-dimethyl-formamide / 4 h / 100 °C / 760.05 Torr
With
1,4-diaza-bicyclo[2.2.2]octane; 1,10-Phenanthroline; oxygen; 18O-labeled water; copper dichloride;
In
N,N-dimethyl-formamide; Petroleum ether;
DOI:10.1021/ol300896h
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Petroleum ether / 10 h / Reflux
2: 1,4-diaza-bicyclo[2.2.2]octane; 1,10-Phenanthroline; oxygen; 18O-labeled water; copper dichloride / N,N-dimethyl-formamide / 4 h / 100 °C / 760.05 Torr
With
1,4-diaza-bicyclo[2.2.2]octane; 1,10-Phenanthroline; oxygen; 18O-labeled water; copper dichloride;
In
N,N-dimethyl-formamide; Petroleum ether;
DOI:10.1021/ol300896h