6^A,6^B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin

Base Information

• Chemical Name: 6^A,6^B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin
• CAS No.: 146099-67-4
• Molecular Formula: C₇₄H₁₁₄O₃₇
• Molecular Weight: 1595.7
• Mol file: 146099-67-4.mol

Synonyms:6^A,6^B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin

Chemical Property of 6^A,6^B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 6^A,6^B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin

There total 2 articles about 6^A,6^B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

C69H106O39S2 + sodium p-(allyloxy)phenoxide → 6A,6B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin (146099-67-4)

Guidance literature:

In N,N-dimethyl-formamide; at 60 ℃;

DOI:10.1016/S0040-4039(00)60062-X

Reference yield:

sodium p-(allyloxy)phenoxide + 6A,6B-bis-O-(2',4'-dimethoxybenzene-1',5'-disulfonyl)-heptakis(2,3-di-O-methyl)-β-cyclodextrin → 6A,6B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin (146099-67-4)

Guidance literature:

In N,N-dimethyl-formamide; for 24h; Yield given; Ambient temperature;

DOI:10.1021/jo960679i

Reference yield: 83.0%

6A,6B-bis-O-heptakis(2,3-di-O-methyl)-β-cyclodextrin (146099-67-4) + methyl iodide (74-88-4) → 6A,6B-bis-O-heptakis(2,3-di-O-methyl)-6C,6D,6E,6F,6G-penta-O-methyl-β-cyclodextrin

Guidance literature:

With sodium iodide; In N,N-dimethyl-formamide; at 0 - 25 ℃;

DOI:10.1016/S0040-4039(00)60062-X