C₅₉H₅₁BrO₄

Base Information

Chemical Name:C₅₉H₅₁BrO₄
CAS No.:363622-87-1
Molecular Formula:C₅₉H₅₁BrO₄
Molecular Weight:903.956
Hs Code.:

C<sub>59</sub>H<sub>51</sub>BrO<sub>4</sub>

Synonyms:C₅₉H₅₁BrO₄

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Chemical Property of C₅₉H₅₁BrO₄

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Technology Process of C₅₉H₅₁BrO₄

There total 10 articles about C₅₉H₅₁BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 363622-81-5
[3,5-Bis-((E)-2-{3,5-bis-[(E)-2-(4-methoxy-phenyl)-vinyl]-phenyl}-vinyl)-phenyl]-methanol

: 363622-87-1
C₅₉H₅₁BrO₄

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In acetonitrile; at 20 ℃;
DOI:10.1021/jo015764r

Reference yield:

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 363622-87-1
C₅₉H₅₁BrO₄

Guidance literature:: Multi-step reaction with 8 steps

1: 33 percent / dimethylformamide / 3 h / 100 °C

2: 100 percent / 4 h / 140 °C

3: t-BuOK / tetrahydrofuran / 20 °C

4: aq. NaOH / 2 h / 20 °C

5: 85 percent / PCC / CH₂Cl₂ / 2 h

6: t-BuOK / tetrahydrofuran / 2 h / 20 °C

7: aq. NaOH / 2 h / 20 °C

8: 90 percent / CBr₄; PPh₃ / acetonitrile / 20 °C

With sodium hydroxide; carbon tetrabromide; potassium tert-butylate; triphenylphosphine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: Arbuzov reaction / 3: Horner-Wadsworth-Emmons reaction / 6: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo015764r

Reference yield:

: 4464-18-0
1,3,5-tris(hydroxymethyl)benzene

: 363622-87-1
C₅₉H₅₁BrO₄

Guidance literature:: Multi-step reaction with 9 steps

1: 90 percent / aq. HBr / acetic acid / 1 h / 20 °C

2: 33 percent / dimethylformamide / 3 h / 100 °C

3: 100 percent / 4 h / 140 °C

4: t-BuOK / tetrahydrofuran / 20 °C

5: aq. NaOH / 2 h / 20 °C

6: 85 percent / PCC / CH₂Cl₂ / 2 h

7: t-BuOK / tetrahydrofuran / 2 h / 20 °C

8: aq. NaOH / 2 h / 20 °C

9: 90 percent / CBr₄; PPh₃ / acetonitrile / 20 °C

With sodium hydroxide; carbon tetrabromide; potassium tert-butylate; hydrogen bromide; triphenylphosphine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile; 3: Arbuzov reaction / 4: Horner-Wadsworth-Emmons reaction / 7: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo015764r