2,3-DICHLORO-5-NITRO-BENZOTRIFLUORIDE

Base Information

• Chemical Name: 2,3-DICHLORO-5-NITRO-BENZOTRIFLUORIDE
• CAS No.: 400-65-7
• Molecular Formula: C7H2Cl2F3NO2
• Molecular Weight: 260.00
• Hs Code.: 2904909090
• Mol file: 400-65-7.mol

Synonyms:1,2-Dichloro-5-nitro-3-(trifluoromethyl)benzene;2,3-Dichloro-5-nitrobenzotrifluoride;

Chemical Property of 2,3-DICHLORO-5-NITRO-BENZOTRIFLUORIDE

Chemical Property:

• Vapor Pressure: 0.0449mmHg at 25°C
• Melting Point: 17-17.5 °C
• Refractive Index: 1.511
• Boiling Point: 245.4 °C at 760 mmHg
• Flash Point: 102.2 °C
• PSA: 45.82000
• Density: 1.638 g/cm³
• LogP: 4.44360
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2,3-Dichloro-5-nitro-benzotrifluoride ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DICHLORO-5-NITRO-BENZOTRIFLUORIDE

There total 1 articles about 2,3-DICHLORO-5-NITRO-BENZOTRIFLUORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-3-(trifluoromethyl)nitrobenzene (777-37-7) → 1,2-dichloro-5-nitro-3-trifluoromethyl-benzene (400-65-7)

Guidance literature:

With antimonypentachloride; chlorine; at 125 ℃;

DOI:10.1021/ja01165a059

Reference yield:

1,2-dichloro-5-nitro-3-trifluoromethyl-benzene (400-65-7) → 3,4-dichloro-5-(trifluoromethyl)aniline (392-90-5)

Guidance literature:

With hydrogenchloride; tin(ll) chloride;

DOI:10.1021/ja01165a059

Reference yield:

1,2-dichloro-5-nitro-3-trifluoromethyl-benzene (400-65-7) → 5-bromo-1,2-dichloro-3-trifluoromethyl-benzene (392-89-2)

Guidance literature:

Multi-step reaction with 2 steps

1: SnCl₂; aqueous HCl

2: sulfuric acid; aqueous sodium nitrite solution / Behandeln der Reaktionsloesung mit Kupfer(I)-bromid

With hydrogenchloride; sulfuric acid; tin(ll) chloride; sodium nitrite;

DOI:10.1021/ja01165a059

upstream raw materials:

4-chloro-3-(trifluoromethyl)nitrobenzene

Downstream raw materials:

3,4-dichloro-5-(trifluoromethyl)aniline

5-bromo-1,2-dichloro-3-trifluoromethyl-benzene

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