3-CHLORO-3',4'-DIFLUOROBENZHYDROL

Base Information

• Chemical Name: 3-CHLORO-3',4'-DIFLUOROBENZHYDROL
• CAS No.: 844683-50-7
• Molecular Formula: C₁₃H₉ClF₂O
• Molecular Weight: 254.664
• Hs Code.: 2906290090
• Mol file: 844683-50-7.mol

Synonyms:(3-chlorophenyl)(3,4-difluorophenyl)methanol

Chemical Property of 3-CHLORO-3',4'-DIFLUOROBENZHYDROL

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3-CHLORO-3',4'-DIFLUOROBENZHYDROL ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

Useful:

Technology Process of 3-CHLORO-3',4'-DIFLUOROBENZHYDROL

There total 1 articles about 3-CHLORO-3',4'-DIFLUOROBENZHYDROL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

(3,4-difluorophenyl)zinc bromide (737797-28-3) + m-Chlorobenzaldehyde (587-04-2) → (3-chlorophenyl)(3,4-difluorophenyl)methanol (844683-50-7)

Guidance literature:

(3,4-difluorophenyl)zinc bromide; With magnesium chloride; In tetrahydrofuran; toluene; at 20 ℃; for 2h; Inert atmosphere;

m-Chlorobenzaldehyde; In tetrahydrofuran; toluene; for 6h; Inert atmosphere;

DOI:10.1021/jo102417x

upstream raw materials:

(3,4-difluorophenyl)zinc bromide

m-Chlorobenzaldehyde

Refernces