3,4-DIFLUOROPHENYLZINC BROMIDE

Base Information

Chemical Name:3,4-DIFLUOROPHENYLZINC BROMIDE
CAS No.:737797-28-3
Molecular Formula:C6H3BrF2Zn
Molecular Weight:258.36900
Hs Code.:2931900090
Mol file:737797-28-3.mol

Synonyms:(3,4-difluorophenyl)-isopropyl-amine;Benzenamine,3,4-difluoro-N-(1-methylethyl);(3,4-difluorophenyl)zinc bromide;

Suppliers and Price of 3,4-DIFLUOROPHENYLZINC BROMIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
3,4-Difluorophenylzinc bromide, 0.5M solution in THF
50 mL
$ 632.00

Rieke Metals
3,4-Difluorophenylzincbromide
100mL
$ 534.00

Rieke Metals
3,4-Difluorophenylzincbromide
50mL
$ 316.00

American Custom Chemicals Corporation
3,4-DIFLUOROPHENYLZINC BROMIDE 95.00%
50ML
$ 2747.47

American Custom Chemicals Corporation
3,4-DIFLUOROPHENYLZINC BROMIDE 95.00%
10ML
$ 1177.11

Alfa Aesar
3,4-Difluorophenylzinc bromide, 0.5M in THF, packaged under Argon in resealable ChemSeal? bottles
50ml
$ 192.00

Total 4 raw suppliers

Chemical Property of 3,4-DIFLUOROPHENYLZINC BROMIDE

Chemical Property:

PSA：0.00000
LogP:2.60810
Sensitive.:Air Sensitive

Purity/Quality:

97% ^*data from raw suppliers

3,4-Difluorophenylzinc bromide, 0.5M solution in THF ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4-DIFLUOROPHENYLZINC BROMIDE

There total 1 articles about 3,4-DIFLUOROPHENYLZINC BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 348-61-8
1-bromo-3,4-difluorobenzene

: 7440-66-6
zinc

: 737797-28-3
(3,4-difluorophenyl)zinc bromide

Guidance literature:: In 2-methyltetrahydrofuran; N,N-dimethyl acetamide; at 120 ℃; for 10h; Inert atmosphere;

Reference yield: 98.0%

: 1007229-67-5
4‐methoxybenzyl 2‐bromopropanoate

: 737797-28-3
(3,4-difluorophenyl)zinc bromide

: (S)-4-methoxybenzyl 2-(3,4-difluorophenyl)propanoate

Guidance literature:: With (4S,4'S)-2,2'-(1,3-bis(4-fluorophenyl)propane-2,2-diyl)bis(4-benzyl-4,5-dihydrooxazole); cobalt(II) iodide; In tetrahydrofuran; at -25 ℃; for 24h; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201705463

Reference yield: 75.0%

: 2404-35-5
cycloheptyl bromide

: 737797-28-3
(3,4-difluorophenyl)zinc bromide

: 1146593-96-5
(3,4-difluorophenyl)cycloheptane

Guidance literature:: (3,4-difluorophenyl)zinc bromide; With (trimethylsilyl)methylmagnesium chloride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;

cycloheptyl bromide; With o-phenylenebis(diphenylphosphine); In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

With iron(III) chloride; In tetrahydrofuran; at 0 - 60 ℃; Inert atmosphere;
DOI:10.1021/jo102417x