C₅₃H₇₀N₄O₁₀

Base Information

Chemical Name:C₅₃H₇₀N₄O₁₀
CAS No.:1613707-34-8
Molecular Formula:C₅₃H₇₀N₄O₁₀
Molecular Weight:923.16
Hs Code.:

C<sub>53</sub>H<sub>70</sub>N<sub>4</sub>O<sub>10</sub>

Synonyms:C₅₃H₇₀N₄O₁₀

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Chemical Property of C₅₃H₇₀N₄O₁₀

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Technology Process of C₅₃H₇₀N₄O₁₀

There total 16 articles about C₅₃H₇₀N₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1613625-27-6
(S)-3-{4-[4-(benzyloxycarbonylamino)but-1-ynyl]naphthalen-1-yl}-2-(tert-butoxycarbonylamino)propanoic acid

: 1613707-33-7
C₂₃H₄₀N₂O₅

: 1613707-34-8
C₅₃H₇₀N₄O₁₀

Guidance literature:: With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

: (Z)-methyl 2-(tert-butyloxycarbonyl)amino-3-(1-(tert-butyldimethylsilyloxy)naphthalen-4-yl)acrylate

: 1613707-34-8
C₅₃H₇₀N₄O₁₀

Guidance literature:: Multi-step reaction with 7 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 20 °C / 760.05 Torr

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

3: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

4: pyridine / 2 h / 0 - 20 °C

5: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

6: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

7: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;

Reference yield:

: 1613707-21-3
methyl 2-(tert-butoxycarbonylamino)-3-(4-(tert-butyldimethylsilyloxy)naphthalen-1-yl)propanoate

: 1613707-34-8
C₅₃H₇₀N₄O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h / 0 °C

2: CHIRAEPAKAD columnS cm I_.Dx₅₀ cm L / isopropyl alcohol; n-heptane / Resolution of racemate

3: pyridine / 2 h / 0 - 20 °C

4: triethylamine; copper(l) iodide; tri-tert-butyl phosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; hexane / 16 h / Inert atmosphere; Reflux

5: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h / 20 °C

6: 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

With pyridine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; water; triethylamine; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; sodium hydroxide; In tetrahydrofuran; methanol; hexane; n-heptane; isopropyl alcohol; acetonitrile;