1-deuterioethylbenzene

Base Information

• Chemical Name: 1-deuterioethylbenzene
• CAS No.: 1861-02-5
• Molecular Formula: C₈H₁₀
• Molecular Weight: 107.159
• Mol file: 1861-02-5.mol

Synonyms:1-deuterioethylbenzene

Chemical Property of 1-deuterioethylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-deuterioethylbenzene

There total 24 articles about 1-deuterioethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(1-bromoethyl)benzne (585-71-7,38661-81-3) → 1-deuterioethylbenzene (1861-02-5)

Guidance literature:

With sodium borodeuteride; cetyltributylphosphonium bromide; In water-d2; toluene; at 18 ℃; for 6h; Product distribution;

DOI:10.1021/jo00332a030

Reference yield: 82.0%

(1-chloroethyl)benzene (672-65-1) → 1-deuterioethylbenzene (1861-02-5)

Guidance literature:

With lithium aluminium deuteride; In tetrahydrofuran; at 0 - 75 ℃; for 20h; Inert atmosphere;

DOI:10.1002/ejoc.201900121

Reference yield:

(R)-1-chloro-1-phenylethane (1459-15-0) → 2,3-diphenylbutane (1857-74-5,2726-21-8,4539-34-8,4613-11-0,71606-46-7,5789-35-5) + ethylbenzene (100-41-4,27536-89-6) + 1-deuterioethylbenzene (1861-02-5) + 2,3-diphenylbutane (4613-11-0,1245924-68-8)

Guidance literature:

(R)-1-chloro-1-phenylethane; With copper; N,N-dimethyl-formamide;

With diclazuril; at -113.15 ℃; for 0.333333h;

DOI:10.1002/poc.964

upstream raw materials:

Et₃SiD

(S)-1-phenylethanol

ethylbenzene

1-Phenylethanol

Downstream raw materials:

ethylbenzene-1,1-d2

1-deuterio-1-phenylethanol

1-Phenylethanol

C₁₄H₁₃⁽²⁾HN₂O₄S