methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

Base Information

Chemical Name:methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate
CAS No.:861857-04-7
Molecular Formula:C₁₅H₂₄N₂O₄
Molecular Weight:296.367
Hs Code.:

Synonyms:methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

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Chemical Property of methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

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Technology Process of methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

There total 2 articles about methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 101558-80-9
methyl2-(2-aminoethylamino)acetate

: 94142-97-9
2-(1-hydroxyethylidene)-5,5-dimethylcyclohexane-1,3-dione

: 861857-04-7
methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; for 15h;
DOI:10.1021/ol049905y

Reference yield: 57.0%

: 94142-97-9
2-(1-hydroxyethylidene)-5,5-dimethylcyclohexane-1,3-dione

: N-(2-aminoethyl)glycine methyl ester dihydrochloride

: 861857-04-7
methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; at 20 ℃; for 16h;
DOI:10.1016/j.tet.2005.06.003

Reference yield: 73.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 861857-04-7
methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate

: 1133971-62-6
N-{2-[1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethylamino]ethyl}-N-(tert-butoxycarbonyl)glycine

Guidance literature:: di-tert-butyl dicarbonate; methyl N-{2-[1-(4,4-dimethyl-2,6-dioxo-cyclohexyliden)-ethylamino]-ethyl}-glycinate; With triethylamine; In tetrahydrofuran; at 20 ℃; for 5h;

With water; caesium carbonate; In methanol; at 20 ℃; for 1.5h;

With potassium hydrogensulfate; In methanol; water; pH=3;
DOI:10.1002/anie.200905699