Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI)
CAS No.:393078-38-1
Molecular Formula:C₁₃H₁₆N₂O₃
Molecular Weight:248.282
Hs Code.:
Mol file:393078-38-1.mol

Synonyms:Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI)

Suppliers and Price of Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-[(2-PYRIDINYLAMINO)CARBONYL]CYCLOHEXANECARBOXYLIC ACID 95.00%
5MG
$ 505.29

Total 1 raw suppliers

Chemical Property of Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI)

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:: 2-[(2-PYRIDINYLAMINO)CARBONYL]CYCLOHEXANECARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI)

There total 2 articles about Cyclohexanecarboxylic acid, 2-[(2-pyridinylamino)carbonyl]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 610-10-6,1687-30-5,2305-32-0,21963-41-7,46022-05-3,610-09-3
(1S,2S)-cyclohexane-1,2-dicarboxylic acid

: 393078-38-1
(1S,2S)-2-(pyridin-2-ylcarbamoyl)cyclohexanecarboxylic acid

: (3aS,7aS)-hexahydro-2-(pyridin-2-yl)-1H-isoindole-1,3(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 5 h / 20 °C

2: triethylamine / dichloromethane / 20 °C / Cooling with ice

With thionyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201400005

Reference yield:

: 46021-27-6
(1S,2S)-cyclohexane-1,2-dicarbonyl dichloride

: 504-29-0
2-aminopyridine

: 393078-38-1
(1S,2S)-2-(pyridin-2-ylcarbamoyl)cyclohexanecarboxylic acid

: (3aS,7aS)-hexahydro-2-(pyridin-2-yl)-1H-isoindole-1,3(2H)-dione

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1002/hlca.201400005 DOI:10.1002/hlca.201400005