1,2-Cyclohexanedicarbonyl dichloride, trans-(-)- (9CI)

Base Information

Chemical Name:1,2-Cyclohexanedicarbonyl dichloride, trans-(-)- (9CI)
CAS No.:46021-27-6
Molecular Formula:C8H10 Cl2 O2
Molecular Weight:209.072
Hs Code.:
Mol file:46021-27-6.mol

Synonyms:1,2-Cyclohexanedicarbonyldichloride, trans-(-)-; trans-(-)-1,2-Cyclohexanedicarbonyl dichloride

Suppliers and Price of 1,2-Cyclohexanedicarbonyl dichloride, trans-(-)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Cyclohexanedicarbonyl dichloride, trans-(-)- (9CI)

Chemical Property:

PSA：34.14000
LogP:2.32360

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-Cyclohexanedicarbonyl dichloride, trans-(-)- (9CI)

There total 4 articles about 1,2-Cyclohexanedicarbonyl dichloride, trans-(-)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 2305-32-0
trans-1,2-cyclohexanedicarboxylic acid

: 33209-25-5,34684-19-0,36909-95-2,46021-27-6,60901-05-5,65653-82-9
trans-1,2-cyclo-hexanedicarboxylic acid dichloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; for 41h;
DOI:10.1021/jo051765y

Reference yield:

: 610-10-6,1687-30-5,2305-32-0,21963-41-7,46022-05-3,610-09-3
(1S,2S)-cyclohexane-1,2-dicarboxylic acid

: 46021-27-6
(1S,2S)-cyclohexane-1,2-dicarbonyl dichloride

Guidance literature:: With thionyl chloride; N,N-dimethyl-formamide; for 41h;
DOI:10.1021/jo051765y

Reference yield:

: 2305-32-0
trans-1,2-cyclohexanedicarboxylic acid

: 46021-27-6
(1S,2S)-cyclohexane-1,2-dicarbonyl dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: 19 percent / (S)-1-phenylethylamine / ethanol; toluene / Heating

2: SOCl₂; DMF / 41 h

With thionyl chloride; (S)-1-phenyl-ethylamine; N,N-dimethyl-formamide; In ethanol; toluene;
DOI:10.1021/jo051765y