4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

Base Information

Chemical Name:4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester
CAS No.:89291-90-7
Molecular Formula:C₅₃H₅₆N₂O₇Si
Molecular Weight:861.122
Hs Code.:

Synonyms:4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

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Chemical Property of 4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

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Technology Process of 4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

There total 4 articles about 4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29576-13-4
methyl 4-hydroxy-2-butenoate

: 89291-90-7
4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole

2: 1.) n-BuLi / 1.) THF, -110 deg C, 2.) -78 deg C

With 1H-imidazole; n-butyllithium;
DOI:10.1016/S0040-4039(00)94158-3

Reference yield:

: 623-43-8
crotonic acid methyl ester

: 89291-90-7
4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: selenium dioxide

2: NaBH₄

3: imidazole

4: 1.) n-BuLi / 1.) THF, -110 deg C, 2.) -78 deg C

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; selenium(IV) oxide;
DOI:10.1016/S0040-4039(00)94158-3

Reference yield:

: 5837-72-9
methyl (E)-4-oxo-2-butenoate

: 89291-90-7
4-(tert-Butyl-diphenyl-silanyloxy)-3-((2S,5S)-1,4-dibenzyl-2,5-bis-benzyloxy-3,6-dioxo-piperazin-2-yl)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄

2: imidazole

3: 1.) n-BuLi / 1.) THF, -110 deg C, 2.) -78 deg C

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium;
DOI:10.1016/S0040-4039(00)94158-3