Technology Process of C14H16O4S
There total 8 articles about C14H16O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzyltriethylammonium tetrathiomolybdate;
In
ethanol; acetonitrile;
at 20 ℃;
for 5h;
enantiospecific reaction;
DOI:10.1002/ejoc.201200906
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium sulfite; sodium disulfite / methanol; water / 3.5 h / 20 °C
2: hydrogenchloride / methanol / 72 h / 20 °C
3: silver(l) oxide / toluene / 1 h / 80 °C / Inert atmosphere
4: silver(l) oxide / toluene / 3.5 h / 80 °C
5: benzyltriethylammonium tetrathiomolybdate / acetonitrile; ethanol / 5 h / 20 °C
With
hydrogenchloride; sodium disulfite; benzyltriethylammonium tetrathiomolybdate; silver(l) oxide; sodium sulfite;
In
methanol; ethanol; water; toluene; acetonitrile;
5: |Michael Addition;
DOI:10.1002/ejoc.201200906
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen bromide; acetic acid / 1 h
2: perchloric acid / 1 h
3: sodium sulfite; sodium disulfite / methanol; water / 3.5 h / 20 °C
4: hydrogenchloride / methanol / 72 h / 20 °C
5: silver(l) oxide / toluene / 1 h / 80 °C / Inert atmosphere
6: silver(l) oxide / toluene / 3.5 h / 80 °C
7: benzyltriethylammonium tetrathiomolybdate / acetonitrile; ethanol / 5 h / 20 °C
With
hydrogenchloride; sodium disulfite; perchloric acid; benzyltriethylammonium tetrathiomolybdate; hydrogen bromide; acetic acid; silver(l) oxide; sodium sulfite;
In
methanol; ethanol; water; toluene; acetonitrile;
7: |Michael Addition;
DOI:10.1002/ejoc.201200906