C₄₄H₆₁FN₆O₄

Base Information

Chemical Name:C₄₄H₆₁FN₆O₄
CAS No.:1009092-03-8
Molecular Formula:C₄₄H₆₁FN₆O₄
Molecular Weight:757.005
Hs Code.:

C<sub>44</sub>H<sub>61</sub>FN<sub>6</sub>O<sub>4</sub>

Synonyms:C₄₄H₆₁FN₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₄H₆₁FN₆O₄

Chemical Property:

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Technology Process of C₄₄H₆₁FN₆O₄

There total 11 articles about C₄₄H₆₁FN₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1009092-12-9
C₄₄H₅₉FN₈O₄

: 1009092-03-8
C₄₄H₆₁FN₆O₄

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; diothiothreitol; In N,N-dimethyl-formamide; for 1h;

Reference yield:

: 149947-15-9
3-bromo-2-fluorobenzaldehyde

: 1009092-03-8
C₄₄H₆₁FN₆O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9

2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

2.2: pH 7

3.1: calcium chloride / diethyl ether / 3 h / 20 °C

4.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation

4.2: 2 h

5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

6.2: 2 h

6.3: 5 h

7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 60 °C

8.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 2 h

9.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; diothiothreitol / N,N-dimethyl-formamide / 1 h

With titanium(IV) isopropylate; hydrogenchloride; potassium hydroxide; hydroxylamine hydrochloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; calcium chloride; diothiothreitol; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 304876-62-8
C₇H₅BrFNO

: 1009092-03-8
C₄₄H₆₁FN₆O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

1.2: pH 7

2.1: calcium chloride / diethyl ether / 3 h / 20 °C

3.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation

3.2: 2 h

4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

5.2: 2 h

5.3: 5 h

6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 2 h / 60 °C

7.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 2 h

8.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; diothiothreitol / N,N-dimethyl-formamide / 1 h

With titanium(IV) isopropylate; hydrogenchloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; calcium chloride; diothiothreitol; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;