methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

Base Information

Chemical Name:methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate
CAS No.:944911-31-3
Molecular Formula:C₃₆H₃₉N₃O₄
Molecular Weight:577.723
Hs Code.:

Synonyms:methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

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Chemical Property of methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

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Technology Process of methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

There total 8 articles about methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₉H₃₃N₃O₄

: 100-52-7
benzaldehyde

: 944911-31-3
methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

Guidance literature:: With Pic-BH₃; In methanol; at 20 ℃; for 14h;
DOI:10.1039/b704366j

Reference yield: 95.0%

: 1219921-29-5
methyl 4-(4-(4-((((9H-fluoren-9-yl)methoxy)carbonyl)(benzyl)amino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

: 944911-31-3
methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

Guidance literature:: With piperidine; In acetonitrile; at 20 ℃; for 14h;
DOI:10.1016/j.tetlet.2009.12.137

Reference yield:

: methyl-4-[N-((4-N-propylamino)benzoyl)-N-isobutylamino]-benzoate

: 944911-31-3
methyl 4-(4-(4-(benzylamino)-N-propylbenzamido)-N-isobutylbenzamido)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / dichlorotriphenylphosphorane / CHCl₃ / 24 h / Heating

2: 60 percent / hydrogen / palladium on charcoal / methanol / 16 h / 20 °C

3: 95 percent / Pic-BH₃ / methanol / 14 h / 20 °C

With hydrogen; dichlorotriphenylphosphorane; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1039/b704366j