1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

Base Information

Chemical Name:1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione
CAS No.:100565-08-0
Molecular Formula:C₂₈H₃₀N₂O₄
Molecular Weight:458.557
Hs Code.:

Synonyms:1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

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Chemical Property of 1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

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Technology Process of 1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

There total 6 articles about 1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100565-06-8
4-Benzyl-3-(bromo-p-tolyl-methyl)-3-methoxy-1-(4-methoxy-benzyl)-piperazine-2,5-dione

: 100565-08-0
1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 24h; Yield given; Ambient temperature; in presence of ammonium acetate;
DOI:10.1246/bcsj.58.1413

Reference yield:

: 100592-97-0
(Z)-1-acetyl-3-(4-methylbenzylidene)-2,5-piperazinedione

: 100565-08-0
1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 5 steps

1: 1) NaH / 1) 30 min, 0 deg C, DMF; 2) 2 h, 0 deg C

2: 92 percent / 70percent hydrazine / dimethylformamide / 3 h / 0 °C

3: 1) NaH / 1) 30 min, 0 deg C, DMF; 2) 2 h, 0 deg C

4: NBS / methanol / 0.5 h / Ambient temperature

5: H₂ / 10percent Pd/C / methanol / 24 h / Ambient temperature; in presence of ammonium acetate

With N-Bromosuccinimide; hydrogen; sodium hydride; hydrazine hydrate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.58.1413

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 100565-08-0
1-benzyl-6-methoxy-4-(4-methoxybenzyl)-6-(4-methylbenzyl)-2,5-piperazinedione

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH / 1) 30 min, 0 deg C, DMF; 2) 2 h, 0 deg C

2: NBS / methanol / 0.5 h / Ambient temperature

3: H₂ / 10percent Pd/C / methanol / 24 h / Ambient temperature; in presence of ammonium acetate

With N-Bromosuccinimide; hydrogen; sodium hydride; palladium on activated charcoal; In methanol;
DOI:10.1246/bcsj.58.1413