Technology Process of C69H94N2O5S8
There total 5 articles about C69H94N2O5S8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
tetrahydrofuran;
for 12h;
Inert atmosphere;
Reflux;
DOI:10.1021/la103686n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / dichloromethane; N,N-dimethyl-formamide
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran
3: methanol; potassium carbonate / dichloromethane
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 12 h / Inert atmosphere; Reflux
With
methanol; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/la103686n
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine / dichloromethane; N,N-dimethyl-formamide
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran
3: methanol; potassium carbonate / dichloromethane
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 12 h / Inert atmosphere; Reflux
With
methanol; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/la103686n