Benzenemethanol, 3-fluoro-2-methoxy- (9CI)

Base Information

• Chemical Name: Benzenemethanol, 3-fluoro-2-methoxy- (9CI)
• CAS No.: 303043-91-6
• Molecular Formula: C8H9 F O2
• Molecular Weight: 156.157
• Hs Code.: 2909499000
• Mol file: 303043-91-6.mol

Synonyms:(3-Fluoro-2-methoxyphenyl)methanol

Chemical Property of Benzenemethanol, 3-fluoro-2-methoxy- (9CI)

Chemical Property:

• Boiling Point: 236.5±25.0 °C(Predicted)
• PKA: 14.09±0.10(Predicted)
• PSA: 29.46000
• Density: 1.187±0.06 g/cm3(Predicted)
• LogP: 1.32660
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Fluoro-2-methoxybenzenemethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3-Fluoro-2-methoxybenzenemethanol

Technology Process of Benzenemethanol, 3-fluoro-2-methoxy- (9CI)

There total 3 articles about Benzenemethanol, 3-fluoro-2-methoxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

fluoro-3 methoxy-2 benzaldehhyde (74266-68-5) → (3-fluoro-2-methoxy-phenyl)-methanol (303043-91-6)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; Inert atmosphere;

Reference yield:

3-fluorosalicylaldehyde (394-50-3) → (3-fluoro-2-methoxy-phenyl)-methanol (303043-91-6)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

With sodium tetrahydroborate; caesium carbonate; In methanol; N,N-dimethyl-formamide;

Reference yield:

→ (3-fluoro-2-methoxy-phenyl)-methanol (303043-91-6)

Guidance literature:

upstream raw materials:

fluoro-3 methoxy-2 benzaldehhyde

3-fluorosalicylaldehyde

Downstream raw materials:

(S)-7-cyano-4-(3-fluoro-2-hydroxybenzyl)-1,2,3,4-tetrahydrocyclopenta[b]indol-2-ylcarbamic acid isopropyl ester

(S)-7-cyano-4-(3-fluoro-2-methoxybenzyl)-1,2,3,4-tetrahydrocyclopenta[b]indol-2-ylcarbamic acid isopropyl ester

1-(Chloromethyl)-3-fluoro-2-methoxy-benzene

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