2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

Base Information

Chemical Name:2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride
CAS No.:1365992-09-1
Molecular Formula:C₁₂H₄Cl₄FIN₂
Molecular Weight:463.892
Hs Code.:

Synonyms:2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

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Chemical Property of 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

Chemical Property:

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Technology Process of 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

There total 5 articles about 2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1365992-08-0
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzamide

: 1365992-09-1
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

Guidance literature:: With thionyl chloride; at 90 ℃; for 56h;

Reference yield:

: 628691-93-0
2-chloro-3-fluoro-pyridine-4-carboxylic acid

: 1365992-09-1
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: diphenyl phosphoryl azide / toluene / 3 h / 110 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

2.2: NH₂ cartridge

3.1: triethylamine / 1,4-dioxane / 18 h / 100 °C

4.1: thionyl chloride / 56 h / 90 °C

With thionyl chloride; diphenyl phosphoryl azide; triethylamine; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; toluene;

Reference yield:

: 1258298-16-6
2,6-dichloro-4-iodo-benzoyl chloride

: 1365992-09-1
2,6-dichloro-N-(2-chloro-3-fluoro-pyridin-4-yl)-4-iodobenzimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 1,4-dioxane / 18 h / 100 °C

2: thionyl chloride / 56 h / 90 °C

With thionyl chloride; triethylamine; In 1,4-dioxane;