N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

Base Information

Chemical Name:N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide
CAS No.:906876-74-2
Molecular Formula:C₂₃H₂₀N₂O₄
Molecular Weight:388.423
Hs Code.:

N<sub>1</sub>-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

Synonyms:N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

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Chemical Property of N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

Chemical Property:

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Technology Process of N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

There total 6 articles about N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 906876-62-8
5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxylic acid

: 100-46-9
benzylamine

: 906876-74-2
N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield:

: 7396-80-7
2-fluoro-2',4-dimethoxybenzophenone

: 906876-74-2
N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium tert-butylate / N,N-dimethyl-formamide / 72 h / 20 °C

2.1: hydrogenchloride / water; acetonitrile / 3 h / 5 - 80 °C

3.1: bromine / chloroform / 1 h / 0 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -70 - 20 °C

5.1: lithium hydroxide; water / methanol / 20 °C

5.2: pH 1

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With hydrogenchloride; lithium hydroxide; n-butyllithium; potassium tert-butylate; water; bromine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 906876-03-7
3-(2,4-dimethoxyphenyl)-1,2-benzisoxazole

: 906876-74-2
N₁-phenylmethyl-5-(1,2-benzisoxazol-3-yl)-2,4-dimethoxybenzenecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine / chloroform / 1 h / 0 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / -70 - 20 °C

3.1: lithium hydroxide; water / methanol / 20 °C

3.2: pH 1

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With lithium hydroxide; n-butyllithium; water; bromine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; hexane; dichloromethane; chloroform;