N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide
CAS No.:1586006-13-4
Molecular Formula:C₁₅H₂₂FNO₃S₂
Molecular Weight:347.475
Hs Code.:

Synonyms:N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

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Chemical Property of N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

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Technology Process of N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

There total 3 articles about N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1191456-53-7
N-(cyclobutylidene)-2-methylpropane-2-sulfinamide

: 20808-12-2
fluoromethyl phenyl sulfone

: 1586006-13-4
N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

Guidance literature:: fluoromethyl phenyl sulfone; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.666667h; Inert atmosphere;

N-(cyclobutylidene)-2-methylpropane-2-sulfinamide; In tetrahydrofuran; at -78 - 20 ℃;

Reference yield:

: 1193-82-4
racemic methyl phenyl sulfoxide

: 1586006-13-4
N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylamino-sulfur trifluoride / chloroform / 20 - 60 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C

With n-butyllithium; diethylamino-sulfur trifluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; chloroform;

Reference yield:

: 60839-94-3
2-fluoro-methylthiobenzene

: 1586006-13-4
N-(1-(fluoro(phenylsulfonyl)methyl)cyclobutyl)-2-methylpropane-2-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;