[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]CF₃SO₃

Base Information

• Chemical Name: [Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]CF₃SO₃
• CAS No.: 69558-38-9
• Molecular Formula: CF₃O₃S*C₄₀H₃₇O₄OsP₂
• Molecular Weight: 982.949

Synonyms:[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]CF₃SO₃

Chemical Property of [Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]CF₃SO₃

Chemical Property:

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Technology Process of [Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]CF₃SO₃

There total 3 articles about [Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]⁽¹⁺⁾*CF₃SO₃^(1-)=[Os(CH₂OCH₃)(H₂O)(CO)2(P(C₆H₅)3)2]CF₃SO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Os(CHO)H(CO)2(P(C6H5)3)2*0.67CH2Cl2 + methyl trifluoromethanesulfonate (333-27-7) → [Os(CH2OCH3)(H2O)(CO)2(P(C6H5)3)2](1+)*CF3SO3(1-)=[Os(CH2OCH3)(H2O)(CO)2(P(C6H5)3)2]CF3SO3 (69558-38-9)

Guidance literature:

With H₂O; In benzene; methyl triflate added to complex soln., stirred for 10 min; pptd. with hexane;

DOI:10.1016/S0022-328X(00)81212-7

Reference yield: 91.6%

Os(CH2O)(CO)2(P(C6H5)3)2*H2O + methyl trifluoromethanesulfonate (333-27-7) → [Os(CH2OCH3)(H2O)(CO)2(P(C6H5)3)2](1+)*CF3SO3(1-)=[Os(CH2OCH3)(H2O)(CO)2(P(C6H5)3)2]CF3SO3 (69558-38-9)

Guidance literature:

In benzene; stirred for 15 min; pptd. with hexane, collected, washed with hexane, recrystd. (CH2Cl2/EtOH/cyclohexane); elem. anal.;

DOI:10.1016/S0022-328X(00)81212-7

Reference yield:

[OsH(CO)3(P(C6H5)3)2](1+)*ClO4(1-)=[OsH(CO)3(P(C6H5)3)2]ClO4 (25838-88-4) → [Os(CH2OCH3)(H2O)(CO)2(P(C6H5)3)2](1+)*CF3SO3(1-)=[Os(CH2OCH3)(H2O)(CO)2(P(C6H5)3)2]CF3SO3 (69558-38-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₄ / ethanol; dichloromethane

2: H₂O / benzene

With NaBH₄; H₂O; In ethanol; dichloromethane; benzene;

DOI:10.1016/S0022-328X(00)81212-7

upstream raw materials:

methyl trifluoromethanesulfonate

[OsH(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsH(CO)3(P(C₆H₅)3)2]ClO₄

Downstream raw materials:

Os(CH₂OCH₃)Cl(CO)2(P(C₆H₅)3)2

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