2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

Base Information

Chemical Name:2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate
CAS No.:1345986-01-7
Molecular Formula:C₂₇H₃₀FNO₆S
Molecular Weight:515.603
Hs Code.:

Synonyms:2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

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Chemical Property of 2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

Chemical Property:

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Technology Process of 2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

There total 9 articles about 2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1174657-32-9
2-(N-tert-butoxycarbonyl-N-(p-methoxybenzyl)amino)-1-phenylethanol

: 349-88-2
4-Fluorobenzenesulfonyl chloride

: 1345986-01-7
2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

Guidance literature:: 2-(N-tert-butoxycarbonyl-N-(p-methoxybenzyl)amino)-1-phenylethanol; With potassium hydroxide; In tetrahydrofuran; for 0.25h;

4-Fluorobenzenesulfonyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: 96-09-3
styrene oxide

: 1345986-01-7
2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: activated silica / 24 h / Inert atmosphere

2: triethylamine / methanol / 0.5 h / Reflux

3: potassium hydroxide / tetrahydrofuran / 0.25 h

With triethylamine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078

Reference yield:

: C₂₁H₂₅NO₄

: 1345986-01-7
2-(tert-butoxycarbonyl(4-methoxybenzyl)amino)-1-phenylethyl 4-fluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 0 °C

2: potassium hydroxide / tetrahydrofuran / 0.25 h

With sodium tetrahydroborate; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2011.08.078