N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide

Base Information

Chemical Name:N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide
CAS No.:175431-36-4
Molecular Formula:C₁₂H₁₅NO₂
Molecular Weight:205.257
Hs Code.:
DSSTox Substance ID:DTXSID101253069
Nikkaji Number:J1.373.009A

Synonyms:175431-36-4;DTXSID101253069;N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide;N-[1-(2-Hydroxyethyl)-2-propen-1-yl]benzamide

Suppliers and Price of N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:205.110278721
Heavy Atom Count:15
Complexity:210

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CC(CCO)NC(=O)C1=CC=CC=C1

Technology Process of N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide

There total 4 articles about N-[1-(2-Hydroxyethyl)-2-propenyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 284670-73-1
ethyl 3-(N-benzoylamino)pent-4-enoate

: 175431-36-4
3-(N-benzoylamino)pent-4-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.25h;
DOI:10.1021/jo000088z

Reference yield:

: 98-88-4
benzoyl chloride

: 175431-36-4
3-(N-benzoylamino)pent-4-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / diethyl ether / 18 h / 0 °C

2: 81 percent / LiAlH₄ / tetrahydrofuran / 0.25 h / 0 - 20 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; diethyl ether; 1: Acylation / 2: Reduction;
DOI:10.1021/jo000088z

Reference yield:

: 4-Vinyl-1,3-oxazin-2-one

: 175431-36-4
3-(N-benzoylamino)pent-4-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 2 M NaOH / ethanol / 2 h / Heating

2: 2 M NaOH / 2.5 h / 0 °C

With sodium hydroxide; In ethanol;