7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione

Base Information

• Chemical Name: 7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione
• CAS No.: 915408-70-7
• Molecular Formula: C₂₇H₃₂FN₃O₃Si
• Molecular Weight: 493.653

Synonyms:7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione

Chemical Property of 7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione

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Technology Process of 7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione

There total 2 articles about 7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

5-amino-7-(4-fluorobenzyl)-9-hydroxy-6H-pyrrolo[3,4-g]quinoline-6,8(7H)-dione hydrochloride (915408-69-4) + triisopropylsilyl chloride (13154-24-0) → 7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione (915408-70-7)

Guidance literature:

With triethylamine; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield: 82.0%

5-amino-7-(4-fluorobenzyl)-9-hydroxy-6H-pyrrolo[3,4-g]quinoline-6,8(7H)-dione (915690-75-4) + triisopropylsilyl chloride (13154-24-0) → 7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione (915408-70-7)

Guidance literature:

With dmap; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1.33333h;

Reference yield: 100.0%

7-(4-fluorobenzyl)-5-amino-9-(triisopropylsilyloxy)-7H-pyrrolo[3,4-g]quinoline-6,8-dione (915408-70-7) + methanesulfonyl chloride (124-63-0) → N-(7-(4-fluorobenzyl)-6,8-dioxo-9-(triisopropylsilyloxy)-7,8-dihydro-6H-pyrrolo[3,4-g]quinolin-5-yl)-N-(methylsulfonyl)methanesulfonamide (915408-71-8)

Guidance literature:

With triethylamine; In dichloromethane; at -5 - 5 ℃; for 2.25 - 2.33333h;

upstream raw materials:

5-amino-7-(4-fluorobenzyl)-9-hydroxy-6H-pyrrolo[3,4-g]quinoline-6,8(7H)-dione

triisopropylsilyl chloride

5-amino-7-(4-fluorobenzyl)-9-hydroxy-6H-pyrrolo[3,4-g]quinoline-6,8(7H)-dione hydrochloride

Downstream raw materials:

N-(7-(4-fluorobenzyl)-6,8-dioxo-9-(triisopropylsilyloxy)-7,8-dihydro-6H-pyrrolo[3,4-g]quinolin-5-yl)-N-(methylsulfonyl)methanesulfonamide

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