(3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

Base Information

Chemical Name:(3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane
CAS No.:949916-62-5
Molecular Formula:C₁₇H₂₆N₂O₄
Molecular Weight:322.404
Hs Code.:

(3S)-N<SUP>1</SUP>-(benzyloxycarbonyl)-N<SUP>3</SUP>-(tert-butyloxycarbonyl)-1,3-diaminobutane

Synonyms:(3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

Suppliers and Price of (3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

There total 1 articles about (3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 176982-57-3,177489-90-6
(3-amino-1(S)-methylpropyl)carbamic acid, 1,1-dimethylethyl ester

: 949916-62-5
(3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

Guidance literature:: at 6 - 20 ℃; for 5h; Alkaline conditions;
DOI:10.1134/S1068162020060126

Reference yield: 75.0%

: 949916-62-5
(3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

: 949916-64-7,1187927-77-0
(S)-N¹-(benzyloxycarbonyl)-1,3-diaminobutane

Guidance literature:: With hydrogenchloride; In ethanol; at 20 ℃; for 3h; enantioselective reaction;
DOI:10.1134/S1068162015050064

Reference yield:

: 949916-62-5
(3S)-N¹-(benzyloxycarbonyl)-N³-(tert-butyloxycarbonyl)-1,3-diaminobutane

: (3S)-N¹-(benzyloxycarbonyl)-N³-(2-nitrophenylsulfonyl)-1,3-diaminobutane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / 3 h / 20 °C

2: triethylamine / dichloromethane / 4 h / 4 - 20 °C

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1134/S1068162015050064