2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

Base Information

Chemical Name:2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid
CAS No.:77192-20-2
Molecular Formula:C₁₈H₂₃O₃PSi
Molecular Weight:346.438
Hs Code.:

Synonyms:2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

Suppliers and Price of 2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

There total 1 articles about 2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 124-38-9,18923-20-1
carbon dioxide

: 63103-39-9
diphenyl[2-(trimethylsilyl)ethyl]phosphine oxide

: 77192-20-2
2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

Guidance literature:: With n-butyllithium; In tetrahydrofuran; 1.) room temperature, 1 h, 2.) -78 deg C to room temperature;
DOI:10.1039/P19810000251

Reference yield: 96.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 77192-20-2
2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

: 77192-21-3
methyl 2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionate

Guidance literature:: In chloroform;
DOI:10.1039/P19810000251

Reference yield:

: 77192-20-2
2-(diphenyloxophosphoranyl)-3-trimethylsilylpropionic acid

: 77192-23-5
6,6-dimethoxy-2-(diphenyloxophosphoranyl)-2-trimethylsilylmethylhexan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / CHCl₃

2: hexamethylphosphoramide, sodium hydride / 64 h / Ambient temperature

3: 74 percent / lithium borohydride / tetrahydrofuran / 72 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium borohydride; sodium hydride; In tetrahydrofuran; chloroform;
DOI:10.1039/P19810000251