oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate

Base Information

Chemical Name:oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate
CAS No.:1417728-61-0
Molecular Formula:C₁₃H₁₄O₆
Molecular Weight:266.251
Hs Code.:

Synonyms:oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate

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Technology Process of oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate

There total 1 articles about oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 99-50-3
3,4-Dihydroxybenzoic acid

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 1417728-59-6
oxiran-2-ylmethyl 3,4-bis(oxiran-2-ylmethoxy)benzoate

: 1417728-61-0
oxiran-2-ylmethyl 3-(hydroxymethyl)-2,3-dihydrobenzo[b][1,4]dioxine-6-carboxylate

Guidance literature:: 3,4-Dihydroxybenzoic acid; epichlorohydrin; With N-benzyl-N,N,N-triethylammonium chloride; at 100 ℃; for 1h;

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; at 30 ℃; for 1.5h;
DOI:10.1016/j.tet.2012.11.079