C₄₄H₆₁NO₁₂

Base Information

Chemical Name:C₄₄H₆₁NO₁₂
CAS No.:245736-74-7
Molecular Formula:C₄₄H₆₁NO₁₂
Molecular Weight:795.968
Hs Code.:

C<sub>44</sub>H<sub>61</sub>NO<sub>12</sub>

Synonyms:C₄₄H₆₁NO₁₂

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Chemical Property of C₄₄H₆₁NO₁₂

Chemical Property:

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Technology Process of C₄₄H₆₁NO₁₂

There total 41 articles about C₄₄H₆₁NO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 245736-65-6
C₄₅H₆₃NO₁₂

: 245736-74-7
C₄₄H₆₁NO₁₂

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile;
DOI:10.1021/ja990789h

Reference yield:

: 245736-63-4
2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

: 245736-74-7
C₄₄H₆₁NO₁₂

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 1,4-cyclohexadiene / 10 percent Pd/C / ethanol

2: 96 percent / 2,4,6-Cl₃PhCOCl, i-Pr₂NEt, DMAP / benzene

3: 99 percent / aq. TsOH / acetonitrile

With dmap; cyclohexa-1,4-diene; 2,4,6-trichlorobenzoyl chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; acetonitrile; benzene;
DOI:10.1021/ja990789h

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 245736-74-7
C₄₄H₆₁NO₁₂

Guidance literature:: Multi-step reaction with 25 steps

1: NaH / dimethylformamide; tetrahydrofuran

2: HCl / methanol; diethyl ether / 0 °C

3: (COCl)2, DMSO, i-Pr₂NEt / -78 - -30 °C

4: 73 percent / TiCl₂(O-i-Pr)2 / CH₂Cl₂ / -78 - 0 °C

5: Et₂BOMe, NaBH₄ / tetrahydrofuran; methanol / -78 °C

6: HCl

7: DIBAL-H / CH₂Cl₂ / -78 °C

8: 1.) Bu₂BOTf, i-Pr₂NEt / 1.) CH₂Cl₂, 0 deg C, 2.) CH₂Cl₂, -78 deg C

9: 100 percent / (COCl)2, DMSO, i-Pr₂NEt / -78 - 0 °C

10: 82 percent / TsOH / acetonitrile / -22 °C

11: 100 percent / (COCl)2, DMSO, Et₃N / -78 - 0 °C

12: LDA / 1 h / -78 °C

13: LiOOH / tetrahydrofuran; dimethylformamide; H₂O / 0 - 23 °C

14: aq. OsO₄, NMO / tetrahydrofuran; 2-methyl-propan-2-ol

15: aq. NaIO₄, NaHCO₃ / tetrahydrofuran; 2-methyl-propan-2-ol

16: 1.) Et₃N, 2.) Et₃NHOAc

17: 1.) c-hex2BCl, Me₂NEt / 1.) Et₂O, 0 deg C, 2.) Et₂O, from -78 deg C to 0 deg C

18: imidazole / CH₂Cl₂

19: Et₃NHOAc

20: (2,4,6-Cl₃PhCO)2O, i-Pr₂NEt, DMAP / benzene

21: 68 percent / 3-ClPhNCO, i-Pr₂NEt / benzene / 90 °C

22: NaHMDS / tetrahydrofuran

23: aq. AgNO₃, 2,6-lutidine / tetrahydrofuran

24: HF*pyr / tetrahydrofuran

25: 99 percent / aq. TsOH / acetonitrile

With 1H-imidazole; 2,6-dimethylpyridine; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; titanium(IV) dichlorodiisopropylate; oxalyl dichloride; lithium hydroperoxide; N,N-dimethyl-ethanamine; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; dicyclohexylboron chloride; sodium hexamethyldisilazane; triethylammonium acetate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; pyridine hydrogenfluoride; silver nitrate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; m-chlorophenyl isocyanate; lithium diisopropyl amide; 2,4,6-trichlorobenzoic anhydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; benzene;
DOI:10.1021/ja990789h