2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

Base Information

Chemical Name:2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester
CAS No.:245736-63-4
Molecular Formula:C₅₂H₇₁NO₁₃
Molecular Weight:918.135
Hs Code.:

2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

Synonyms:2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

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Chemical Property of 2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

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Technology Process of 2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

There total 1 articles about 2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₄H₉₉NO₁₃Si₂

: 245736-63-4
2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

Guidance literature:: With 2,6-dimethylpyridine; pyridine hydrogenfluoride;
DOI:10.1021/ja990789h

Reference yield: 100.0%

: 245736-63-4
2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

: 245736-64-5
2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid

Guidance literature:: With cyclohexa-1,4-diene; palladium on activated charcoal; In ethanol;
DOI:10.1021/ja990789h

Reference yield:

: 245736-63-4
2-{6-[4-hydroxy-9-{3-[4-hydroxy-3-methyl-6-(2-methyl-propenyl)-tetrahydro-pyran-2-ylmethyl]-isoxazol-5-yl}-1-(4-methoxy-benzyloxy)-5-methyl-6-oxo-decyl]-2-methoxy-4-methoxycarbonylmethylene-tetrahydro-pyran-2-yl}-propionic acid benzyl ester

: 245736-65-6
C₄₅H₆₃NO₁₂

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 1,4-cyclohexadiene / 10 percent Pd/C / ethanol

2: 96 percent / 2,4,6-Cl₃PhCOCl, i-Pr₂NEt, DMAP / benzene

With dmap; cyclohexa-1,4-diene; 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1021/ja990789h