C₁₂H₁₉NO₃S

Base Information

• Chemical Name: C₁₂H₁₉NO₃S
• CAS No.: 1431555-59-7
• Molecular Formula: C₁₂H₁₉NO₃S
• Molecular Weight: 257.354
• Mol file: 1431555-59-7.mol

Synonyms:C₁₂H₁₉NO₃S

Chemical Property of C₁₂H₁₉NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₂H₁₉NO₃S

There total 1 articles about C₁₂H₁₉NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isocyanate de chlorosulfonyle (1189-71-5) + 3,3-dimethyl-1-phenyl-2-butanol (105735-62-4,105735-63-5,148152-05-0,50695-92-6) → C12H19NO3S (1431555-59-7)

Guidance literature:

isocyanate de chlorosulfonyle; With formic acid; In dichloromethane; at 0 - 20 ℃; for 9h;

3,3-dimethyl-1-phenyl-2-butanol; With pyridine; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/ja3122526

Reference yield: 81.0%

C12H19NO3S (1431555-59-7) → C12H17NO3S (1431555-69-9) + C12H17NO3S (1431555-74-6)

Guidance literature:

With [bis(acetoxy)iodo]benzene; [Fe^II(2,2’:6’,2’’:6’’,2’’’:6’’’,2’’’’-quinquepyridine)(CH3CN)₂](ClO₄)₂; magnesium oxide; In acetonitrile; at 80 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ja3122526

upstream raw materials:

isocyanate de chlorosulfonyle

3,3-dimethyl-1-phenyl-2-butanol

Downstream raw materials:

C₁₂H₁₇NO₃S

C₁₂H₁₇NO₃S

Refernces