(2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

Base Information

Chemical Name:(2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate
CAS No.:134390-24-2
Molecular Formula:C₁₇H₁₉NO₅S
Molecular Weight:349.408
Hs Code.:

Synonyms:(2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

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Chemical Property of (2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

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Technology Process of (2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

There total 3 articles about (2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5194-51-4
(2E,4E)-hexa-2,4-diene

: 134390-15-1
methyl 2-<(2-nitrophenyl)sulfinyl>-2,3-butadienoate

: 134390-24-2
(2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

Guidance literature:: In dichloromethane; at 23 ℃; for 2h; under 8250660 Torr;
DOI:10.1021/jo00013a033

Reference yield:

: 31555-05-2
methyl 4-hydroxy-2-butynoate

: 134390-24-2
(2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / CH₂Cl₂ / 0.17 h / -95 °C

2: 88 percent / CH₂Cl₂ / 2 h / 23 °C / 8250660 Torr

With triethylamine; In dichloromethane;
DOI:10.1021/jo00013a033

Reference yield:

: 7669-54-7
2-nitrobenzenesulfenyl chloride

: 134390-24-2
(2-carbomethoxy-3,6-dimethyl-1,4-cyclohexadienyl)methyl 2-nitrobenzenesulfenate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / CH₂Cl₂ / 0.17 h / -95 °C

2: 88 percent / CH₂Cl₂ / 2 h / 23 °C / 8250660 Torr

With triethylamine; In dichloromethane;
DOI:10.1021/jo00013a033