1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

Base Information

Chemical Name:1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one
CAS No.:1264084-85-6
Molecular Formula:C₁₈H₁₃ClN₂O₂
Molecular Weight:324.766
Hs Code.:

Synonyms:1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

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Technology Process of 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

There total 2 articles about 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1264084-72-1
C₁₉H₁₅ClO₄

: 1264084-85-6
1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

Guidance literature:: With acetic acid; hydrazine; In 2-ethoxy-ethanol; for 20h; Reflux;
DOI:10.1007/s10593-010-0637-4

Reference yield:

: 142917-39-3
(6-methyl-1-benzofuran-3-yl)acetic acid

: 1264084-85-6
1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / 48 h

2.1: aluminum (III) chloride / dichloromethane / 3 h / 25 - 30 °C

2.2: Cooling with ice

3.1: acetic acid; hydrazine / 2-ethoxy-ethanol / 20 h / Reflux

With aluminum (III) chloride; acetic acid; acetyl chloride; hydrazine; In 2-ethoxy-ethanol; dichloromethane;
DOI:10.1007/s10593-010-0637-4