1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione

Base Information

• Chemical Name: 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione
• CAS No.: 1332479-82-9
• Molecular Formula: C₁₈H₁₃ClN₂OS
• Molecular Weight: 340.833

Synonyms:1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione

Chemical Property of 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione

There total 1 articles about 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one (1264084-85-6) → 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione (1332479-82-9)

Guidance literature:

With Lawessons reagent; In toluene; at 100 ℃; for 2h;

DOI:10.1007/s00706-011-0500-z

Reference yield: 90.0%

1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione (1332479-82-9) + 4-methoxybenzoic acid hydrazide (3290-99-1) → 6-(4-chlorophenyl)-3-(4-methoxyphenyl)-9-methyl-12H-[1]benzofuro-[3,2-e][1,2,4]triazolo[4,3-b][1,2]diazepine (1332479-84-1)

Guidance literature:

In butan-1-ol; for 20h; Reflux;

DOI:10.1007/s00706-011-0500-z

Reference yield: 87.0%

1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione (1332479-82-9) + 4-chlorobenzoic acid hydrazide (536-40-3) → 3,6-bis(4-chlorophenyl)-9-methyl-12H-[1]benzofuro-[3,2-e][1,2,4]triazolo[4,3-b][1,2]diazepine (1332479-83-0)

Guidance literature:

In butan-1-ol; for 20h; Reflux;

DOI:10.1007/s00706-011-0500-z

upstream raw materials:

1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-one

Downstream raw materials:

6-(4-chlorophenyl)-9-methyl-3-(pyridin-4-yl)-12H-[1]benzofuro[3,2-e][1,2,4]triazolo[4,3-b][1,2]diazepine

6-(4-chlorophenyl)-3-(4-methoxyphenyl)-9-methyl-12H-[1]benzofuro-[3,2-e][1,2,4]triazolo[4,3-b][1,2]diazepine

3,6-bis(4-chlorophenyl)-9-methyl-12H-[1]benzofuro-[3,2-e][1,2,4]triazolo[4,3-b][1,2]diazepine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1332479-82-9 1-(4-chlorophenyl)-3,5-dihydro-8-methyl-4H-[1]benzofuro[2,3-d][1,2]diazepine-4-thione

Send

Send

Metric Ton KG G Pound L ML

Send

Send